1-羟基环己烷丙酸 gamma-内酯合成路线 （共 73 条）
反应条件
3 A molecular sieve; pyridinium chlorochromate in dichloromethane
8 h; Heating;
参考文献
Baskaran, S.; Chandrasekaran, S.
Tetrahedron Letters, 1990 , vol. 31, # 19 p. 2775 - 2778
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Baskaran, Sundarababu; Islam, Imadul; Chandrasekaran, Srinivasan
Journal of Chemical Research, Miniprint, 1992 , p. 2213 - 2246
反应条件
sulfuric acid in methanol
24 h; Heating;
参考文献
Crotti, Paolo; Badalassi, Fabrizio; Di Bussolo, Valeria; Favero, Lucilla; Pineschi, Mauro
Tetrahedron, 2001 , vol. 57, # 40 p. 8559 - 8572
反应条件
amberlyst-15 in benzene
36 h; Heating; Yields of byproduct given;
参考文献
Bunce, Richard A.; Drumright, Raymond E.; Taylor, Vicki L.
Synthetic Communications, 1989 , vol. 19, # 13-14 p. 2423 - 2430
参考文献
Linstead; Millidge; Walpole
Journal of the Chemical Society, 1937 , p. 1140,1145
反应条件
chloro-trimethyl-silane; sodium iodide in acetonitrile
T=60°C;
参考文献
Piva, Olivier
Tetrahedron, 1994 , vol. 50, # 48 p. 13687 - 13696
反应条件
cerium in tetrahydrofuran
2 h; Ambient temperature;
参考文献
Fukuzawa, Shin-ichi; Fujinami, Tatsuo; Sakai, Shizuyoshi
Journal of the Chemical Society, Chemical Communications, 1986 , # 6 p. 475 - 476
反应条件
in formic acid
24 h; Heating;
参考文献
Edward, John T.; Cooke, Ellen; Paradellis, Themistocles C.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 597 - 600
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide in tetrahydrofuran; tert-butyl alcohol
Ambient temperature;
参考文献
Csuk; Hu; Abdou; Kratky
Tetrahedron, 1991 , vol. 47, # 34 p. 7037 - 7044
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide; methyl 3-bromo-propionate in tetrahydrofuran
Ambient temperature;
参考文献
Csuk; Hu; Abdou; Kratky
Tetrahedron, 1991 , vol. 47, # 34 p. 7037 - 7044
反应条件
1: ethyl bromoacetate With Bu6CrLi3 in tetrahydrofuran
T=-78 - -20°C; 1 h;
2: methylidenecyclohexane oxide With triethylaluminum in tetrahydrofuran
T=-78 - 25°C; 2 h; Title compound not separated from byproducts;
参考文献
Hojo, Makoto; Sakata, Kyosuke; Maimaiti, Xiamuxikamaer; Ueno, Junya; Nishikori, Hisashi; Hosomi, Akira
Chemistry Letters, 2002 , # 2 p. 142 - 143
