in gaseous matrix Defluorination in N2 atmosphere (flow rate 4l/h) at 560 °C/760 Torr.;
参考文献
Burdon, J.; Gilman, D. J.; Patrick, C. R.; Stacey, M.; Tatlow, J. C.
Nature (London, United Kingdom), 1960 , vol. 186, p. 231 - 232
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Gmelin Handbook: F: PerFHalOrg.5, 4, page 115 - 148
KF-KCl melt in neat (no solvent) Fluorination at 740 .degree C., yields of C5FnCl5-nN (n= 1 to 5) are indicated for the fluorination of the temperature range 630 - 740 °C;;
参考文献
Hitzke, J.; Guion, J.
Bulletin de la Societe Chimique de France, 1974 , p. 811 - 814
KF-KCl melt in neat (no solvent) Inlet of the formed C5F3Cl2N (3g/10 min) at 645 °C into the KF-KCl melt (carrier gas = Ar, flow rate 70 ml/min), yields of C5FnCl5-nN (n= 1 to 5) are indicated for the fluorination of the temperature range 630 - 740 °C;;
