4-甲氧基苯甲酰基氟化物合成路线 （共 32 条）
反应条件
XeF2 in dichloromethane
3 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Nongkunsarn, Pakawan; Ramsden, Christopher A.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 2 p. 121 - 122
反应条件
1: hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; 1,2-bis-(diphenylphosphino)ethane / chlorobenzene / 3 h / Inert atmosphere; Reflux
2: hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; 1,2-bis-(diphenylphosphino)ethane / chlorobenzene / 9 h / Inert atmosphere; Reflux
3: hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; cis-DPPEthylene / chlorobenzene / 2 h / Inert atmosphere; Reflux
View Scheme
参考文献
Arisawa, Mieko; Igarashi, Yui; Kobayashi, Haruki; Yamada, Toru; Bando, Kentaro; Ichikawa, Takuya; Yamaguchi, Masahiko
Tetrahedron, 2011 , vol. 67, # 40 p. 7846 - 7859
反应条件
in water
T=25°C; ionic strengh 1.0 (KCl), 0.2M potassium phosphate buffer; Rate constantMechanism;
参考文献
Song, Byeong Doo; Jencks, William P.
Journal of the American Chemical Society, 1989 , vol. 111, # 22 p. 8479 - 8484
反应条件
in water
T=25°C; ionic strengh 1.0 (KCl), 0.2M potassium phosphate buffer, various pH; Rate constantMechanism;
参考文献
Song, Byeong Doo; Jencks, William P.
Journal of the American Chemical Society, 1989 , vol. 111, # 22 p. 8479 - 8484
反应条件
in dichloromethane
T=0 - 20°C; 2.25 h;
参考文献
White, Jonathan M.; Tunoori, Ashok Rao; Turunen, Brandon J.; Georg, Gunda I.
Journal of Organic Chemistry, 2004 , vol. 69, # 7 p. 2573 - 2576
反应条件
triethylamine in N,N-dimethyl-formamide
T=20°C; Inert atmosphere;
参考文献
Ueda, Tsuyoshi; Konishi, Hideyuki; Manabe, Kei
Organic Letters, 2013 , vol. 15, # 20 p. 5370 - 5373
反应条件
in water
T=25°C; Rate constant;
参考文献
Song, Byeong Doo; Jencks, William P.
Journal of the American Chemical Society, 1989 , vol. 111, # 22 p. 8470 - 8479
反应条件
in water
T=25°C; ionic strengh 1.0 (KCl), 0.2M potassium phosphate buffer; Rate constantMechanism;
参考文献
Song, Byeong Doo; Jencks, William P.
Journal of the American Chemical Society, 1989 , vol. 111, # 22 p. 8479 - 8484
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; 1,2-bis-(diphenylphosphino)ethane in chlorobenzene
3 h; Inert atmosphereReflux;
参考文献
Arisawa, Mieko; Igarashi, Yui; Kobayashi, Haruki; Yamada, Toru; Bando, Kentaro; Ichikawa, Takuya; Yamaguchi, Masahiko
Tetrahedron, 2011 , vol. 67, # 40 p. 7846 - 7859
反应条件
1: hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; 1,2-bis-(diphenylphosphino)ethane / chlorobenzene / 3 h / Inert atmosphere; Reflux
2: hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; oxygen; 1,2-bis-(diphenylphosphino)ethane / chlorobenzene / 9 h / Air atmosphere; Reflux
View Scheme
参考文献
Arisawa, Mieko; Igarashi, Yui; Kobayashi, Haruki; Yamada, Toru; Bando, Kentaro; Ichikawa, Takuya; Yamaguchi, Masahiko
Tetrahedron, 2011 , vol. 67, # 40 p. 7846 - 7859
