5,5-二甲基-3-(甲胺)-2-环己烯-1-酮合成路线 （共 6 条）
反应条件
in methanol
T=10°C; preparative electrolysis, 0.1 M NaClO4, 6 F/Mol, graphite anode at 1.00 V;
参考文献
Schaefer, Hans J.; Ellenberg, Wolf
Heterocycles, 1989 , vol. 28, # 2 p. 979 - 985
反应条件
ethylenediaminetetraacetic acid; Mercury
参考文献
Moehrle, Hans; Herbke, Juergen
Monatshefte fuer Chemie, 1980 , vol. 111, p. 627 - 634
反应条件
sodium hydride
1.)toluene,reflux,3 h 2.)1 eq iodomethane,reflux,1-2 h; Yield given. Multistep reaction;
参考文献
Greenhill, John V.; Moten, Ashraf M.
Tetrahedron, 1983 , vol. 39, # 20 p. 3405 - 3408
反应条件
sodium hydride
1.)THF,reflux,1 h 2.)2 eq iodomethane,reflux,1-2 h; Yield given. Multistep reaction;
参考文献
Greenhill, John V.; Moten, Ashraf M.
Tetrahedron, 1983 , vol. 39, # 20 p. 3405 - 3408
反应条件
sodium hydride in 1,4-dioxane
HeatingEffect of solvents, ratio of reagents and reflux period. Other enaminones were also investigated.; Product distribution;
参考文献
Greenhill, John V.; Moten, Ashraf M.
Tetrahedron, 1983 , vol. 39, # 20 p. 3405 - 3408
反应条件
in toluene
168 h; Heating;
参考文献
Kascheres, Concetta; Kascheres, Albert; Pilli, Paula S. H.
Journal of Organic Chemistry, 1980 , vol. 45, # 26 p. 5340 - 5343
