1: 1-bromo-2-methyl benzene With n-butyllithium in tetrahydrofuran
T=-78°C; 1 h; Sealed tubeInert atmosphere;
2: zinc(II) chloride in tetrahydrofuran
T=-78 - 20°C; Sealed tubeInert atmosphere;
参考文献
Dennis, Joseph M.; Calyore, Catherine M.; Sjoholm, Jessica S.; Lutz, J. Patrick; Gair, Joseph J.; Johnson, Jeffrey B.
Synlett, 2013 , vol. 24, # 19 art. no. ST-2013-S0592-L, p. 2567 - 2570
in xylene
on react. of diaryl mercury compd. with Zn wool in anhyd. xylene;;
参考文献
Kozeschkow, K. A.; Nesmeyanow, A. N.; Potrosov, W. I.
Ber., 1934 , vol. 67, p. 1138 - 1142
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Gmelin Handbook: Zn: SVol., 177, page 555 - 558
