9-(4-吗啉基)-1,2,3,4-四氢吖啶合成路线 （共 5 条）
反应条件
phenol
T=80 - 130°C; 8 h;
参考文献
Tripathi; Verma; Pandey, Jyoti; Agarwal; Chaturvedi, Vinita; Manju; Srivastva; Gaikwad; Sinha
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 19 p. 5144 - 5147
反应条件
1: 65 percent / POCl3 / toluene / 8 h / 20 - 100 °C
2: 60 percent / phenol / 8 h / 80 - 130 °C
View Scheme
参考文献
Tripathi; Verma; Pandey, Jyoti; Agarwal; Chaturvedi, Vinita; Manju; Srivastva; Gaikwad; Sinha
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 19 p. 5144 - 5147
反应条件
1: 90 percent / IR-120 resin / toluene / 5 h / Heating
2: 65 percent / POCl3 / toluene / 8 h / 20 - 100 °C
3: 60 percent / phenol / 8 h / 80 - 130 °C
View Scheme
参考文献
Tripathi; Verma; Pandey, Jyoti; Agarwal; Chaturvedi, Vinita; Manju; Srivastva; Gaikwad; Sinha
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 19 p. 5144 - 5147
反应条件
1: 90 percent / IR-120 resin / toluene / 5 h / Heating
2: 65 percent / POCl3 / toluene / 8 h / 20 - 100 °C
3: 60 percent / phenol / 8 h / 80 - 130 °C
View Scheme
参考文献
Tripathi; Verma; Pandey, Jyoti; Agarwal; Chaturvedi, Vinita; Manju; Srivastva; Gaikwad; Sinha
Bioorganic and Medicinal Chemistry Letters, 2006 , vol. 16, # 19 p. 5144 - 5147
反应条件
1: phosphoryl chloride
2: copper-powder
View Scheme
参考文献
Sargent; Small
Journal of Organic Chemistry, 1946 , vol. 11, p. 359,360, 361
