反应条件
Na in ammonia
NH3 (liquid); inert atmosphere; Na addn. to Ph2BiCl, then addn. of excess Fe(CO)5, stirring and evapn. (3 h), washing (hexane); dissoln. in CH2Cl2, filtration, solvent removal (vac.), extn. (hexane), concn., crystn. of Ph4Bi2 and (Ph2Bi)2Fe(CO)4; residue remaining after extn. dissolved in CH2Cl2, filtration, concn., pptn. of (PhBiFe(CO)4)2 on cooling; elem. anal.;
参考文献
Cassidy, Juanita M.; Whitmire, Kenton H.
Inorganic Chemistry, 1991 , vol. 30, p. 2788 - 2795
