N-(叔丁基)-2-氯苯甲酰胺合成路线 (共 4 条)
反应条件
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine in tetrahydrofuran T=20°C;
参考文献
AbbVie Inc.; Abbott GmbH and Co. KG; Geneste, Hervé; OCHSE, Michael; DRESCHER, Karla; TURNER, Sean; BEHL, Berthold; LAPLANCHE, Loic; DINGES, Jürgen; JAKOB, Clarissa; BLACK, Lawrence
Patent: US2013/116233 A1, 2013 ;
Location in patent: Paragraph 1094; 1095 ;
反应条件
Ce(IV)-incorporated sulfated zirconia T=110°C; Ritter reaction; 5 h; neat (no solvent);
参考文献
Kahandal, Sandeep S.; Kale, Sandip R.; Disale, Shamrao T.; Jayaram, Radha V.
Chemistry Letters, 2012 , vol. 41, # 7 p. 738 - 740
反应条件
sulfated tungstate T=100°C; Ritter reaction; 3 h; Neat (no solvent);
参考文献
Katkar, Kamlesh V.; Chaudhari, Pramod S.; Akamanchi, Krishnacharya G.
Green Chemistry, 2011 , vol. 13, # 4 p. 835 - 838
反应条件
sodium hydroxide in water
参考文献
Bayer Aktiengesellschaft
Patent: US4496736 A1, 1985 ;