反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -78 °C / |Schlenk technique; |Inert atmosphere
1.2: -90 - 20 °C / |Schlenk technique; |Inert atmosphere
2.1: palladium diacetate; dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; potassium carbonate / neat (no solvent) / 24 h / 110 °C / |Schlenk technique; |Inert atmosphere
View Scheme
参考文献
Asachenko, Andrey F.; Sorochkina, Kristina R.; Dzhevakov, Pavel B.; Topchiy, Maxim A.; Nechaev, Mikhail S.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 18 p. 3553 - 3557
