2,2-二氟-3,3-双(三氟甲基)环氧乙烷合成路线 （共 6 条）
参考文献
Knunyants,I.L. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1968 , p. 405 - 407
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1968 , # 2 p. 415 - 417
反应条件
in diethyl ether T=-78°C; 2 h; Heating;
参考文献
Kadyrov, A. A.; Bargamov, G. G.; Rokhlin, E. M.
Journal of Fluorine Chemistry, 1993 , vol. 65, # 3 p. 195 - 202
反应条件
T=20°C; 1 h; Further byproducts given;
参考文献
Kadyrov, A. A.; Rokhlin, E. M.; Knunyats, I. L.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 11 p. 2210
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 11 p. 2653
反应条件
dimethyl benzene-1,4-dicarboxylate in ethylene glycol dimethyl ether
T=20°C; 14 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Kadyrov, A. A.; Rokhlin, E. M.; Knunyants, I. L.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 10 p. 2063 - 2066
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 10 p. 2344 - 2347
反应条件
in diethyl ether
T=-78°C; 2 h;
参考文献
Kadyrov, A. A.; Bargamov, G. G.; Rokhlin, E. M.
Journal of Fluorine Chemistry, 1993 , vol. 65, # 3 p. 195 - 202
反应条件
(i), (ii) KOH, (iii) (heating); Multistep reaction;
参考文献
Bekker,R.A. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1978 , vol. 27, p. 1462 - 1463
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1978 , vol. 27, # 7 p. 1672 - 1673
