O,O’-二乙基-(2-琥珀酸二乙酯基)膦酸酯合成路线 (共 21 条)
反应条件
1: 40 percent / NaOEt / ethanol / 1.5 h / ice bath 2: 61 percent / PCl3 / CHCl3 / 3 h / Heating View Scheme
参考文献
Kadin, Saul B.; Lamphere, Charles H.
Journal of Organic Chemistry, 1984 , vol. 49, # 25 p. 4999 - 5000
反应条件
sodium hydride in tetrahydrofuran; paraffin
1 h; Ambient temperature;
参考文献
Okauchi, Tatsuo; Fukamachi, Takeshi; Nakamura, Fumio; Ichikawa, Junji; Minami, Toru
Bulletin des Societes Chimiques Belges, 1997 , vol. 106, # 9-10 p. 525 - 532
反应条件
potassium carbonate; tetrabutylammomium bromide
T=70 - 80°C; 4 h;
参考文献
Makosza, Mieczyslaw; Wojciechowski, Krzysztof
Bulletin of the Polish Academy of Sciences, Chemistry, 1984 , vol. 32, # 3-6 p. 175 - 179
反应条件
potassium carbonate in ethanol
T=28°C; Addition; Pudovik reaction; 1 h;
参考文献
Platonov; Sivakov; Chistokletov; Maiorova
Russian Journal of General Chemistry, 1999 , vol. 69, # 3 p. 493 - 494
反应条件
1: H2O (excess) / toluene
2: 90 °C / 16 Torr
View Scheme
参考文献
Caesar, Julian C.; Griffiths, D. Vaughan; Griffiths, Penelope A.; Tebby, John C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 8 p. 2329 - 2334
参考文献
Caesar, Julian C.; Griffiths, D. Vaughan; Griffiths, Penelope A.; Tebby, John C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 8 p. 2329 - 2334
反应条件
1: HBr-gas / toluene / 0 °C
2: 90 °C / 16 Torr
View Scheme
参考文献
Caesar, Julian C.; Griffiths, D. Vaughan; Griffiths, Penelope A.; Tebby, John C.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , # 8 p. 2329 - 2334
参考文献
Harvey,R.G.
Tetrahedron, 1966 , vol. 22, p. 2561 - 2573
反应条件
ethanol; sodium ethanolate
参考文献
Pudowik
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1952 , p. 926,928
Chem.Abstr., 1953 , p. 10467
Show Details
Union Carbide and Carbon Corp.
Patent: US2754315 , 1948 ;
反应条件
P=0.001 Torr; Heating;
参考文献
Pudovik,A.N. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1975 , vol. 45, p. 272 - 275,257 - 259