2-羟基-3-苯基-2-环己酮合成路线 （共 24 条）
反应条件
sodium acetate; palladium diacetate; ethylene glycol; poly(ethylene glycol) in water; acetonitrile
T=150°C; 0.333333 h; microwave irradiation;
参考文献
Svennebring, Andreas; Garg, Neeraj; Nilsson, Peter; Hallberg, Anders; Larhed, Mats
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4720 - 4725
反应条件
sodium acetate; palladium diacetate; ethylene glycol; poly(ethylene glycol) in water; acetonitrile
T=150°C; 0.333333 h; microwave irradiation;
参考文献
Svennebring, Andreas; Garg, Neeraj; Nilsson, Peter; Hallberg, Anders; Larhed, Mats
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4720 - 4725
反应条件
sodium acetate; palladium diacetate; ethylene glycol; poly(ethylene glycol) in water; acetonitrile
T=150°C; 0.333333 h; microwave irradiation;
参考文献
Svennebring, Andreas; Garg, Neeraj; Nilsson, Peter; Hallberg, Anders; Larhed, Mats
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4720 - 4725
反应条件
palladium diacetate; ethylene glycol; N-ethyl-N,N-diisopropylamine; poly(ethylene glycol) in water; acetonitrile
T=150°C; 0.333333 h; microwave irradiation;
参考文献
Svennebring, Andreas; Garg, Neeraj; Nilsson, Peter; Hallberg, Anders; Larhed, Mats
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4720 - 4725
反应条件
acetic acid
0.5 h; to 50 deg C;
参考文献
Feigenbaum, Alexandre; Pete, Jean-Pierre; Scholler, Denise
Journal of Organic Chemistry, 1984 , vol. 49, # 13 p. 2355 - 2360
反应条件
1: iPr2NEt / acetonitrile / 3 h / 100 °C
2: sodium acetate; palladium acetate; poly(ethylene glycol) / acetonitrile; H2O / 0.33 h / 150 °C / microwave irradiation
View Scheme
参考文献
Svennebring, Andreas; Garg, Neeraj; Nilsson, Peter; Hallberg, Anders; Larhed, Mats
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4720 - 4725
反应条件
1: sodium acetate; palladium acetate; poly(ethylene glycol) / acetonitrile; H2O / 0.33 h / 150 °C / microwave irradiation
View Scheme
参考文献
Svennebring, Andreas; Garg, Neeraj; Nilsson, Peter; Hallberg, Anders; Larhed, Mats
Journal of Organic Chemistry, 2005 , vol. 70, # 12 p. 4720 - 4725
反应条件
1: 18 percent / diethyl ether / 0.5 h / Irradiation
2: 63 percent / diethyl ether; methanol / Irradiation; other α-sulfonyloxyenones; other solvent: MeCN, addition of quenchers and sensibilisators
View Scheme
参考文献
Feigenbaum, Alexandre; Pete, Jean-Pierre; Scholler, Denise
Journal of Organic Chemistry, 1984 , vol. 49, # 13 p. 2355 - 2360
反应条件
in methanol; diethyl ether
5 h; Irradiation;
参考文献
Feigenbaum, Alexandre; Pete, Jean-Pierre; Scholler, Denise
Journal of Organic Chemistry, 1984 , vol. 49, # 13 p. 2355 - 2360
反应条件
triethylamine
1. THF, -78 deg C; room temperature, 135 min.; diethylether, pH8, 2. CH2Cl2, room temperature, 4h; Yield given. Multistep reaction;
参考文献
Charonnat; Mitchell; Keogh
Tetrahedron Letters, 1990 , vol. 31, # 3 p. 315 - 318
