1,2-二甲氧基-4-硝基苯合成路线 (共 111 条)
反应条件
(-)-N,N,α-trimethylbenzylamine; water
T=20°C; Reduction; substitution; 1 h; Irradiation;
参考文献
Mir, Miquel; Marquet, Jordi; Massot, Oriol
Tetrahedron, 1999 , vol. 55, # 43 p. 12603 - 12614
反应条件
water
T=20°C; Substitution; reduction; 1 h; Irradiation;
参考文献
Mir, Miquel; Marquet, Jordi; Massot, Oriol
Tetrahedron, 1999 , vol. 55, # 43 p. 12603 - 12614
反应条件
water; 1-amino diphenylmethane
T=20°C; Reduction; substitution; 1 h; Irradiation;
参考文献
Mir, Miquel; Marquet, Jordi; Massot, Oriol
Tetrahedron, 1999 , vol. 55, # 43 p. 12603 - 12614
反应条件
water
T=20°C; Substitution; reduction; 1 h; Irradiation; Further byproducts given;
参考文献
Mir, Miquel; Marquet, Jordi; Massot, Oriol
Tetrahedron, 1999 , vol. 55, # 43 p. 12603 - 12614
反应条件
methanol; sodium methylate
参考文献
Robinson
Journal of the Chemical Society, 1917 , vol. 111, p. 117
反应条件
water
T=20°C; Substitution; reduction; 1 h; Irradiation;
参考文献
Mir, Miquel; Marquet, Jordi; Massot, Oriol
Tetrahedron, 1999 , vol. 55, # 43 p. 12603 - 12614
反应条件
triethylamine in acetonitrile
Ambient temperatureIrradiation; Rate constantProduct distributionMechanism;
参考文献
Gonzalez-Blanco, Roberto; Bourdelande, Jose L.; Marquet, Jordi
Journal of Organic Chemistry, 1997 , vol. 62, # 20 p. 6903 - 6910
反应条件
in methanol; water
4 h; Ambient temperatureIrradiation;
参考文献
Cervello, J.; Figueredo, M.; Marquet, J.; Moreno-Manas, M.; Bertran, J.; Lluch, J. M.
Tetrahedron Letters, 1984 , vol. 25, # 37 p. 4147 - 4150
反应条件
in water; acetonitrile
8 h; IrradiationpH 11, other pH,; Product distribution;
参考文献
Kuzmic, Petr; Pavlickova, Libuse; Velek, Jiri; Soucek, Milan
Collection of Czechoslovak Chemical Communications, 1986 , vol. 51, # 8 p. 1665 - 1670
反应条件
1: 95 percent / conc. H2SO4, KNO3 / 0.5 h / -5 - 0 °C
2: H2 / 10percent Pd/C / methanol / Ambient temperature
3: methanol / 21 h / Ambient temperature
View Scheme
参考文献
Alcalde, E; Dinares, I; Frigola, J
European Journal of Medicinal Chemistry, 1991 , vol. 26, # 6 p. 633 - 642