反应条件
Li in butan-1-ol Li was dissolved in BuOH at room temp. under N2; phthalonitrile was added; stirred at 75°C for 14 min; CuCl2 was added; reacted for 30 min; poured into H2O/MeOH (2/1); filtered; dissolved in CH2Cl2; dried (Na2SO4); evapd. (vac.); chromd. (alumina, CH2Cl2); concd. (vac., below 40°C); hexane added; elem. anal.;
参考文献
Fukuda, Takamitsu; Kikukawa, Yuu; Tsuruya, Ryota; Fuyuhiro, Akira; Ishikawa, Naoto; Kobayashi, Nagao
Inorganic Chemistry, 2011 , vol. 50, # 22 p. 11832 - 11837
