2-烯丙氧基-4-甲氧基苯甲醛合成路线 （共 6 条）
反应条件
sodium hydroxide; (benzyl)-tri-(butyl)-ammonium chloride in dichloromethane
Ambient temperature;
参考文献
Rohlmann, Renate; Daniliuc, Constantin-Gabriel; Mancheno, Olga Garcia
Chemical Communications, 2013 , vol. 49, # 99 p. 11665 - 11667
反应条件
pyridinium chlorochromate in dichloromethane
T=20°C; 4 h;
参考文献
Li, Yang; Jardine, Katherine J.; Tan, Runyu; Song, Datong; Dong, Vy M.
Angewandte Chemie - International Edition, 2009 , vol. 48, # 51 p. 9690 - 9692
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere
2: pyridinium chlorochromate / dichloromethane / 4 h / 20 °C
View Scheme
参考文献
Li, Yang; Jardine, Katherine J.; Tan, Runyu; Song, Datong; Dong, Vy M.
Angewandte Chemie - International Edition, 2009 , vol. 48, # 51 p. 9690 - 9692
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 20 °C
2: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere
3: pyridinium chlorochromate / dichloromethane / 4 h / 20 °C
View Scheme
参考文献
Li, Yang; Jardine, Katherine J.; Tan, Runyu; Song, Datong; Dong, Vy M.
Angewandte Chemie - International Edition, 2009 , vol. 48, # 51 p. 9690 - 9692
反应条件
nachfolgend Kochen mit Wasser;
参考文献
Sonn; Patschke
Chemische Berichte, 1925 , vol. 58, p. 1702
反应条件
1: zinc / N,N-dimethyl-formamide; tetrahydrofuran / 20 °C
2: Jone's reagent / acetone / 0 °C
3: silver nitrate / acetonitrile / 1.5 h / 80 °C
4: water / 60 - 150 °C / |Microwave irradiation
5: dihydrogen peroxide / water; ethanol / 40 - 80 °C / |Microwave irradiation
View Scheme
参考文献
He, Yan; Zhang, Xinying; Cui, Liangyan; Wang, Jianji; Fan, Xuesen
Green Chemistry, 2012 , vol. 14, # 12 p. 3429 - 3435
