2-氯-1,2-双-(4-甲氧基苯基)-乙酮合成路线 (共 7 条)
反应条件
4-methoxy pyridine; Ru(bpy)3Cl2; sodium carbonate in N,N-dimethyl acetamide T=25°C; 48 h; Irradiation;
参考文献
Su, Yijin; Zhang, Liangren; Jiao, Ning
Organic Letters, 2011 , vol. 13, # 9 p. 2168 - 2171
反应条件
potassium carbonate in acetone 3 h; Heating;
参考文献
Tetrahedron, , vol. 44, # 16 p. 5189 - 5198
反应条件
thionyl chloride; N,N-dimethyl-formamide in diethyl ether
0.5 h; Ambient temperature;
参考文献
Karavan, V. S.; Simonov, D. A.
Journal of Organic Chemistry USSR (English Translation), 1989 , vol. 25, # 1.2 p. 145 - 148
Zhurnal Organicheskoi Khimii, 1989 , vol. 25, # 1 p. 159 - 164
反应条件
1: trichloromonobromomethane With triphenylphosphine in dichloromethane
T=20°C; Appel reaction; 0.666667 h; in air;
2: 4,4'-bismethoxybenzoin in dichloromethane
T=20°C; Appel reaction; in air;
参考文献
Newman, Stephen G.; Bryan, Christopher S.; Perez, Didier; Lautens, Mark
Synthesis, 2011 , # 2 art. no. Z27210SS, p. 342 - 346
反应条件
thionyl chloride; benzene
参考文献
Henne; Bruylants
Bulletin des Societes Chimiques Belges, 1948 , vol. 57, p. 320,328
参考文献
Dodds et al.
Proceedings of the Royal Society of London, Series B: Biological Sciences, 1945 , vol. 132, p. 83,95
参考文献
Henne; Bruylants
Bulletin des Societes Chimiques Belges, 1948 , vol. 57, p. 320,328
Show Details
Foeldi; Demjen
Chemische Berichte, 1941 , vol. 74, p. 930,933