4,5-二氢-2-苯基恶唑合成路线 （共 96 条）
反应条件
1: 15 percent / Et3N / acetonitrile / RT, 2 h, then reflux, 10 h 2: 60 percent / nitromethane / 12 h / 60 - 70 °C 3: 70 percent / acetonitrile / RT, 2 h, then reflux, 6 h View Scheme
参考文献
Tetrahedron, , vol. 42, # 5 p. 1449 - 1460
反应条件
1: 65 percent / 4 h / Heating 2: 60 percent / nitromethane / 12 h / 60 - 70 °C 3: 70 percent / acetonitrile / RT, 2 h, then reflux, 6 h View Scheme
参考文献
Tetrahedron, , vol. 42, # 5 p. 1449 - 1460
反应条件
1.1: polymer-NMe3(+) I(N3)2(-) / dichloromethane / 24 h / |Darkness 1.2: 4 h / 20 °C 2.1: benzene / 20 °C / |Flow reactor; |UV-irradiation View Scheme
参考文献
Beilstein Journal of Organic Chemistry, , vol. 9, p. 1745 - 1750
反应条件
sodium hydride in acetonitrile 56 h; Ambient temperature;
参考文献
Ikeda, Katsuya; Honda, Hiroyuki; Matsuo, Takanori; Yamamoto, Tamotsu
Organic Preparations and Procedures International, 1995 , vol. 27, # 1 p. 103 - 106
反应条件
in acetonitrile 8 h;
参考文献
Singh, Harjit; Sarin, Rakesh
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 81 - 82
反应条件
sodium T=20°C; 336000 h;
参考文献
Guthrie, J. Peter; Gallant, Roger T.; Jennings, Michael C.
Canadian Journal of Chemistry, 2004 , vol. 82, # 2 p. 268 - 278
反应条件
bromine in acetonitrile 1 h; Ambient temperature;
参考文献
Goosen, Andre; McCleland, Cedric W.; Sipamla, Allworth M.
Journal of Chemical Research, Miniprint, 1995 , # 10 p. 2221 - 2232
反应条件
in acetonitrile 10 h;
参考文献
Singh, Harjit; Sarin, Rakesh
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1986 , vol. 25, p. 81 - 82
参考文献
Chemische Berichte, , vol. 35, p. 166
Chemische Berichte, , vol. 25, p. 2387
反应条件
triethylamine 120 h; Ambient temperature;
参考文献
Chemische Berichte, , vol. 114, # 11 p. 3599 - 3608
