2,5-二溴-1,5-己二烯合成路线 （共 7 条）
反应条件
1: With 9-bromo-9-borabicyclononane in dichloromethane
T=0°C; Suzuki Coupling; 3 h; Inert atmosphere;
2: With acetic acid in dichloromethane
T=0°C; 1 h; Inert atmosphere;
参考文献
Wang, Huan; Predeus, Alexander V.; Wulff, William D.
Chemistry - A European Journal, 2013 , vol. 19, # 25 p. 8261 - 8267
反应条件
potassium tert-butylate in ethanol
0.166667 h; Heating;
参考文献
Hammad, Loubna A.; Wenthold, Paul G.
Journal of the American Chemical Society, 2003 , vol. 125, # 36 p. 10796 - 10797
反应条件
1: Br2 / CCl4 / 20 °C
2: potassium tert-butoxide / ethanol / 0.17 h / Heating
View Scheme
参考文献
Hammad, Loubna A.; Wenthold, Paul G.
Journal of the American Chemical Society, 2003 , vol. 125, # 36 p. 10796 - 10797
反应条件
in diethyl ether
2 h; Heating;
参考文献
Peterson, Paul E.; Nelson, David J.; Risener, Rick
Journal of Organic Chemistry, 1986 , vol. 51, # 12 p. 2381 - 2382
反应条件
1: Br2 / CCl4
2: NaOEt / ethanol
View Scheme
参考文献
Kira, Mitsuo; Hino, Takakazu; Kubota, Yasushi; Matsuyama, Naoko
Tetrahedron Letters, 1988 , vol. 29, # 52 p. 6939 - 6942
反应条件
in benzene
T=25°C; Irradiationphotholysis of 2,3-diazobicyclo<2.2.2>oct-2-ene derivatives; fluorescence quantum yields and lifetimes, effect of temperature, rate constant for fluorescence; Quantum yield;
参考文献
Engel, Paul S.; Horsey, Douglas W.; Keys, Dalen E.; Nalepa, Christopher J.; Soltero, Luis R.
Journal of the American Chemical Society, 1983 , vol. 105, # 24 p. 7108 - 7114
反应条件
in N,N-dimethyl-formamide
T=130°C;
参考文献
Hammad, Loubna A.; Wenthold, Paul G.
Journal of the American Chemical Society, 2003 , vol. 125, # 36 p. 10796 - 10797
Title/Abstract Full Text View citing articles Show Details
Chacko, Silvi A.; Wenthold, Paul G.
Journal of Organic Chemistry, 2007 , vol. 72, # 2 p. 494 - 501
