2-(2-甲氧基-2-氧代乙基)苯羧酸甲酯合成路线 (共 48 条)
反应条件
Ambient temperatureIrradiation;
参考文献
Journal of Organic Chemistry, , vol. 58, # 7 p. 1976 - 1984
反应条件
(i) Et2O, (ii) /BRN= 1098229/, PhCO2Ag, Et3N; Multistep reaction;
参考文献
Journal of the Chemical Society, , p. 3579 - 3582
反应条件
1 h; Irradiation; Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 36, # 5 p. 677 - 680
反应条件
1: sodium; diethyl ether / Erwaermen des Reaktionsprodukts auf 100grad. 2: aqueous hydrochloric acid View Scheme
参考文献
Johnston et al.
Journal of Organic Chemistry, 1948 , vol. 13, p. 477,482
反应条件
1.1: n-butyllithium; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere 1.2: 13 h / -78 - 20 °C / Inert atmosphere 2.1: potassium hydroxide / methanol; water / 1 h / Reflux View Scheme
参考文献
Billamboz, Muriel; Bailly, Fabrice; Lion, Cedric; Calmels, Christina; Andreola, Marie-Line; Witvrouw, Myriam; Christ, Frauke; Debyser, Zeger; De Luca, Laura; Chimirri, Alba; Cotelle, Philippe
European Journal of Medicinal Chemistry, 2011 , vol. 46, # 2 p. 535 - 546
参考文献
Duggleby,P.McC.; Holt,G.
Journal of the Chemical Society, 1962 , p. 3579 - 3582
反应条件
T=105°C; 20 h; other solvents, reaction time and temperature, effects of the reactants ratio and of the presence of H2O or TFAA; Product distribution;
参考文献
Tabor, Derrick C.; Evans, Slayton A.; Kenan, William Rand
Synthetic Communications, 1982 , vol. 12, # 11 p. 855 - 864
反应条件
T=105°C; 20 h; other solvents, reaction time and temperature, effects of the reactants ratio and of the presence of H2O or TFAA; Product distribution;
参考文献
Tabor, Derrick C.; Evans, Slayton A.; Kenan, William Rand
Synthetic Communications, 1982 , vol. 12, # 11 p. 855 - 864
反应条件
methanol; sodium amide; benzene weiteres Reagens: H2SO4; Erhitzen des Reaktionsprodukts mit Palladium/Kohle und anschliessendes Hydrolysieren;
参考文献
Loewenthal; Pappo
Journal of the Chemical Society, 1952 , p. 4799,4803
反应条件
T=105°C; 20 h; other solvents, reaction time and temperature, effects of the reactants ratio and of the presence of H2O or TFAA; Product distribution;
参考文献
Tabor, Derrick C.; Evans, Slayton A.; Kenan, William Rand
Synthetic Communications, 1982 , vol. 12, # 11 p. 855 - 864