1,3,5-三异丙基苯合成路线 (共 123 条)
反应条件
hierarchical zeolite T=349.84°C; 3 h; Product distribution; Further Variations:Reagentstime;
参考文献
Odedairo; Balasamy; Al-Khattaf
Journal of Molecular Catalysis A: Chemical, 2011 , vol. 345, # 1-2 p. 21 - 36
反应条件
silica-supported P,Mo catalyst T=250°C; atmospheric pressure; Product distribution; Further Variations:Catalysts;
参考文献
Shi, Chunfeng; Wang, Runwei; Zhu, Guangshan; Qiu, Shilun; Long, Jun
European Journal of Inorganic Chemistry, 2006 , # 15 p. 3054 - 3060
反应条件
1: With 2-hydroxy-1,3-isoindolinedione; 2,2'-azo-bisisobutyronitrile; oxygen in acetonitrile T=75°C; P=760 Torr; 2 h; 2: With sulfuric acid in acetonitrile T=20°C; 2 h; Title compound not separated from byproducts;
参考文献
Aoki, Yasuhiro; Hirai, Naruhisa; Sakaguchi, Satoshi; Ishii, Yasutaka
Tetrahedron, 2005 , vol. 61, # 46 p. 10995 - 10999
反应条件
1: oxygen; aqueous Na2CO3 / 85 °C 2: aqueous HClO4; acetic acid; methanol View Scheme
参考文献
Hooker Electrochem. Co.
Patent: US2790010 , 1952 ;
反应条件
carbon disulfide; aluminium trichloride
参考文献
Fuson et al.
Journal of the American Chemical Society, 1942 , vol. 64, p. 2573,2575
反应条件
2-hydroxy-1,3-isoindolinedione; 2,2'-azo-bisisobutyronitrile; oxygen in acetonitrile T=75°C; P=760 Torr; 2 h; Title compound not separated from byproducts;
参考文献
Seidel et al.
Journal fuer Praktische Chemie (Leipzig), 1956 , vol. <4> 3, p. 278,297
Full Text Show Details
Wolkow; Sawgorodnii
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 3672,3676; engl. Ausg. S. 3630, 3633
Full Text Show Details
Wolkow
Chimija chim. Technol.Chem.Abstr., (NDVS) 1959 311 1950 , p. 21774
反应条件
1: With 2-hydroxy-1,3-isoindolinedione; 2,2'-azo-bisisobutyronitrile; oxygen in acetonitrile T=75°C; P=760 Torr; 2 h; 2: With sulfuric acid in acetonitrile T=20°C; 2 h; Title compound not separated from byproducts;
参考文献
Aoki, Yasuhiro; Hirai, Naruhisa; Sakaguchi, Satoshi; Ishii, Yasutaka
Tetrahedron, 2005 , vol. 61, # 46 p. 10995 - 10999
反应条件
nitric acid; acetic anhydride; acetic acid T=0°C; 2 h;
参考文献
Liu, Jing-Yu; Zheng, Yi; Li, Yan-Guo; Pan, Li; Li, Yue-Sheng; Hu, Ning-Hai
Journal of Organometallic Chemistry, 2005 , vol. 690, # 5 p. 1233 - 1239
参考文献
Newton
Journal of the American Chemical Society, 1943 , vol. 65, p. 2444
反应条件
1-(p-toluenebenzenesulfonyloxy)-1,2-benziodoxol-3(1H)-on; tetrabutylammomium bromide in acetonitrile 16 h; Ambient temperatureother reagents (trivalent iodine compounds + LiBr or Bu4NBr), other reagent ratio; Product distribution;
参考文献
Muraki, Takahito; Togo, Hideo; Yokoyama, Masataka
Journal of Organic Chemistry, 1999 , vol. 64, # 8 p. 2883 - 2889