1,1,1,3,3,3-六氟代-2-苯基-2-丙醇合成路线 （共 34 条）
反应条件
DPPH-H in chloroform-d1 T=-78°C; chemiluminescence, other peroxides; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 102, # 10 p. 3515 - 3524
参考文献
Journal of the American Chemical Society, , vol. 95, # 6 p. 2017 - 2019
反应条件
tetrakis(dimethylamino)ethylene in N,N-dimethyl-formamide T=-20 - 20°C; 2 h;
参考文献
Tetrahedron Letters, , vol. 43, # 24 p. 4317 - 4319
反应条件
DPPH-H in chloroform-d1 T=-75°C; chemiluminescence, other peroxides; Product distributionMechanism;
参考文献
Journal of the American Chemical Society, , vol. 102, # 10 p. 3515 - 3524
反应条件
sodium hexamethyldisilazane in tetrahydrofuran T=-100°C;
参考文献
Hartkopf, Uwe; Meijere, Armin de
Angewandte Chemie, 1982 , vol. 94, # 6 p. 444
参考文献
Journal of the American Chemical Society, , vol. 97, # 21 p. 6137 - 6144
反应条件
in tetrahydrofuran T=0 - 20°C; Cannizzaro-type reaction; Inert atmosphere;
参考文献
Dalton Transactions, , vol. 39, # 41 p. 9823 - 9829
反应条件
1: 86 percent / 1,3-dicyclohexylcarbodiimide / dioxane / 1 h / 20 °C 2: 81 percent / tetramethylammonium fluoride / 1,2-dimethoxy-ethane / -30 - 20 °C View Scheme
参考文献
Tetrahedron, , vol. 61, # 7 p. 1813 - 1819
反应条件
1: 98 percent Spectr. / TDAE / 1,2-dimethoxy-ethane / 2 h / -20 - 20 °C 2: 100 percent Spectr. / NaOH / methanol; H2O / Heating View Scheme
参考文献
Tetrahedron Letters, , vol. 43, # 24 p. 4317 - 4319
反应条件
sodium hydroxide in N,N-dimethyl-formamide T=20°C; Cannizzaro-type reaction; 10 h; Inert atmosphere;
参考文献
Dalton Transactions, , vol. 39, # 41 p. 9823 - 9829
