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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
71993-33-4
合成路线
（共 14 条）
71993-33-4
→
反应条件
10173-84-9
反应条件
potassium hydroxide in ethanol 2 h; Heating;
参考文献
Sahasrabhuddhe; Ghiya
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 1 p. 61 - 63
4143-72-0
1-(1-羟基苯基)-3-(4-甲氧基苯基)丙烷-1,3-二酮
→
反应条件
71993-33-4
反应条件
1: With sulfuric acid; ammonium chloride; dihydrogen peroxide; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane; water 3 h; 2: With toluene-4-sulfonic acid in dimethyl sulfoxide T=50 - 60°C; 1 h;
参考文献
Makrandi; Shashi; Kumar, Surender
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 4 p. 895 - 896
4143-74-2
4--甲氧基黄酮
→
反应条件
71993-33-4
反应条件
pyridine; chloro-trimethyl-silane; [bis(acetoxy)iodo]benzene in dichloromethane T=0°C; 3 h;
参考文献
Ho Sik Rho; Ko; Ju
Synthetic Communications, 2001 , vol. 31, # 14 p. 2101 - 2106
767303-58-2
→
反应条件
71993-33-4
反应条件
N-chloro-succinimide in N,N-dimethyl-formamide T=100°C; 2 h;
参考文献
Lin, Chi-Fong; Duh, Tsai-Hui; Lu, Wen-Der; Lee, Jeng-Lin; Lee, Chia-Ying; Chen, Chin-Chau; Wu, Ming-Jung
Journal of the Chinese Chemical Society, 2004 , vol. 51, # 1 p. 183 - 186
3327-24-0
2'-羟基-2-(4-甲氧基亚苄基)乙酰苯
→
反应条件
71993-33-4
反应条件
copper(II) chloride-DMSO 2 h; Heating;
参考文献
Sahasrabhuddhe; Ghiya
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 1 p. 61 - 63
4143-72-0
1-(1-羟基苯基)-3-(4-甲氧基苯基)丙烷-1,3-二酮
→
反应条件
71993-33-4
反应条件
sulfuric acid; ammonium chloride; dihydrogen peroxide; tetra(n-butyl)ammonium hydrogensulfate in dichloromethane; water 3 h;
参考文献
Makrandi; Shashi; Kumar, Surender
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2004 , vol. 43, # 4 p. 895 - 896
89-95-2
2-甲基苯甲醇
→
反应条件
71993-33-4
反应条件
1: 92 percent / dimethylformamide / 12 h / 25 °C 2: 86 percent / BuLi / tetrahydrofuran / 2 h / 0 °C 3: 95 percent / MnO2 / CH2Cl2 / 25 °C 4: 60 percent / N-chlorosuccinimide / dimethylformamide / 2 h / 100 °C View Scheme
参考文献
Lin, Chi-Fong; Duh, Tsai-Hui; Lu, Wen-Der; Lee, Jeng-Lin; Lee, Chia-Ying; Chen, Chin-Chau; Wu, Ming-Jung
Journal of the Chinese Chemical Society, 2004 , vol. 51, # 1 p. 183 - 186
135-02-4
2-甲氧基苯甲醛
→
反应条件
71993-33-4
反应条件
1: 86 percent / BuLi / tetrahydrofuran / 2 h / 0 °C 2: 95 percent / MnO2 / CH2Cl2 / 25 °C 3: 60 percent / N-chlorosuccinimide / dimethylformamide / 2 h / 100 °C View Scheme
参考文献
Lin, Chi-Fong; Duh, Tsai-Hui; Lu, Wen-Der; Lee, Jeng-Lin; Lee, Chia-Ying; Chen, Chin-Chau; Wu, Ming-Jung
Journal of the Chinese Chemical Society, 2004 , vol. 51, # 1 p. 183 - 186
768-60-5
4-乙炔基苯甲醚
→
反应条件
71993-33-4
反应条件
1: 86 percent / BuLi / tetrahydrofuran / 2 h / 0 °C 2: 95 percent / MnO2 / CH2Cl2 / 25 °C 3: 60 percent / N-chlorosuccinimide / dimethylformamide / 2 h / 100 °C View Scheme
参考文献
Lin, Chi-Fong; Duh, Tsai-Hui; Lu, Wen-Der; Lee, Jeng-Lin; Lee, Chia-Ying; Chen, Chin-Chau; Wu, Ming-Jung
Journal of the Chinese Chemical Society, 2004 , vol. 51, # 1 p. 183 - 186
767303-68-4
→
反应条件
71993-33-4
反应条件
1: 95 percent / MnO2 / CH2Cl2 / 25 °C 2: 60 percent / N-chlorosuccinimide / dimethylformamide / 2 h / 100 °C View Scheme
参考文献
Lin, Chi-Fong; Duh, Tsai-Hui; Lu, Wen-Der; Lee, Jeng-Lin; Lee, Chia-Ying; Chen, Chin-Chau; Wu, Ming-Jung
Journal of the Chinese Chemical Society, 2004 , vol. 51, # 1 p. 183 - 186
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