(E)-2-丁烯基乙酸酯合成路线 (共 41 条)
反应条件
[Pd2(dibenzylideneacetone)3]*dibenzylideneacetone; triphenylphosphine in chloroform-d1
T=20°C; 1 h;
参考文献
Braddock; Wildsmith, Andrew J
Tetrahedron Letters, 2001 , vol. 42, # 18 p. 3239 - 3242
反应条件
[(PPh3)3Pd] in N,N-dimethyl-formamide
T=120°C; 5 h;
参考文献
Inoue, Yoshio; Taguchi, Masaaki; Toyofuku, Masanori; Hashimoto, Harukichi
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 10 p. 3021 - 3022
反应条件
tetrakis(triphenylphosphine) palladium(0); chiral biphosphino ligand in tetrahydrofuran
Ambient temperature; Yields of byproduct given;
参考文献
Eichelmann, Holger; Gais, Hans-Joachim
Tetrahedron: Asymmetry, 1995 , vol. 6, # 3 p. 643 - 646
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
3 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Negishi, Ei-ichi; Chatterjee, Sugata; Matsushita, Hajime
Tetrahedron Letters, 1981 , vol. 22, # 38 p. 3737 - 3740
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
3 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Negishi, Ei-ichi; Chatterjee, Sugata; Matsushita, Hajime
Tetrahedron Letters, 1981 , vol. 22, # 38 p. 3737 - 3740
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
12 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Negishi, Ei-ichi; Chatterjee, Sugata; Matsushita, Hajime
Tetrahedron Letters, 1981 , vol. 22, # 38 p. 3737 - 3740
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
24 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Negishi, Ei-ichi; Chatterjee, Sugata; Matsushita, Hajime
Tetrahedron Letters, 1981 , vol. 22, # 38 p. 3737 - 3740
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
3 h; Ambient temperature; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Negishi, Ei-ichi; Chatterjee, Sugata; Matsushita, Hajime
Tetrahedron Letters, 1981 , vol. 22, # 38 p. 3737 - 3740
反应条件
copper (I) cyanide; triphenylphosphine
1.) THF, Et2O (or Et2O-pentane), 0 deg C, 20 min 2.) Et2O (or Et2O-pentane), 0 deg C, 2-4 h; Yield given. Multistep reaction;
参考文献
Fleming, Ian; Higgins, Dick; Lawrence, Nicholas J.; Thomas, Andrew P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 24 p. 3331 - 3350
反应条件
Si{CH2CH2Si[CH2CH2SiCH3(CH2PPh2)2PdMeCl]3}4 in dichloromethane
T=20°C; 1 h; Product distribution; Further Variations:Catalysts;
参考文献
De Groot, Debby; Reek, Joost N. H.; Kamer, Paul C. J.; Van Leeuwen, Piet W. N. M.
European Journal of Organic Chemistry, 2002 , # 6 p. 1085 - 1095