(2S,4S)-(+)-戊二醇合成路线 （共 36 条）
反应条件
sodium hydroxide; hydrogen T=212°C; P=51716.2 Torr; Product distribution / selectivity;
参考文献
ARCHER-DANIELS-MIDLAND COMPANY
Patent: WO2008/133939 A1, 2008 ;
Location in patent: Page/Page column 18-19; 25 ;
反应条件
sodium hydroxide; hydrogen T=209 - 213°C; P=51716.2 - 82745.9 Torr; Product distribution / selectivity;
参考文献
ARCHER-DANIELS-MIDLAND COMPANY
Patent: WO2008/133939 A1, 2008 ;
Location in patent: Page/Page column 18-19; 25 ;
反应条件
samarium diiodide; water in tetrahydrofuran T=20°C; 0.141667 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 53, # 8 p. 1017 - 1020
反应条件
sodium hydroxide; hydrogen T=196°C; P=82745.9 Torr; Product distribution / selectivity;
参考文献
WO2008/133939 A1, ;
Page/Page column 18; 24 ;
反应条件
sodium hydroxide; hydrogen T=193 - 211°C; P=82745.9 Torr; Product distribution / selectivity;
参考文献
WO2008/133939 A1, ;
Page/Page column 18; 24 ;
反应条件
sodium hydroxide; hydrogen T=177 - 228°C; P=62059.4 - 82745.9 Torr; Product distribution / selectivity;
参考文献
WO2008/133939 A1, ;
Page/Page column 18; 24 ;
反应条件
hydrogen; L-(+)-tartaric acid; nickel; sodium bromide in acetic acid T=100°C; P=33752.7 Torr; 18 h; enantio-/diastereoselctivity; dependence on catalyst, time, temperature, pH; Product distribution;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 100, # 8 p. 571 - 584
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride; magnesium iodide 1.) toluene, ether, -60 deg C, 2-5 h, 2.) 70 deg C, 1-2 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 48, # 8 p. 1531 - 1538
参考文献
Chemische Berichte, , vol. 37, p. 4730
Monatshefte fuer Chemie, , vol. 27, p. 1108
反应条件
(i) Hg(OAc)2, H2O, (ii) NaBH4; Multistep reaction;
参考文献
Bulletin de la Societe Chimique de France, , p. 1946 - 1949
