(4-甲酰基苯基)磷酸二乙酯合成路线 （共 8 条）
反应条件
1: NH3; ZnI2 2: pyridine 3: 85 percent / 20 percent aq. HCl / 3 h / 100 °C View Scheme
参考文献
Gasparini, Fabrizio; Inderbitzin, Werner; Francotte, Eric; Lecis, Gabrielle; Richert, Paul; Dragic, Zorica; Kuhn, Rainer; Flor, Peter J.
Bioorganic and Medicinal Chemistry Letters, 2000 , vol. 10, # 11 p. 1241 - 1244
反应条件
tetrakis(triphenylphosphine) palladium(0); triethylamine
T=130°C; 21 h; Green chemistry;
参考文献
Wang, Ping; Lu, Jie; Zhang, Zhan-Hui
Journal of Chemical Research, 2013 , vol. 37, # 6 p. 359 - 361
反应条件
1: With 2-fluoro-pyridine; trifluoromethylsulfonic anhydride in dichloromethane
T=-78 - 0°C; Inert atmosphere;
2: With triethylsilane in dichloromethane
T=0 - 25°C; Inert atmosphere;
3: With citric acid in tetrahydrofuran; dichloromethane; water
T=45°C; 2 h; chemoselective reaction;
参考文献
Pelletier, Guillaume; Bechara, William S.; Charette, Andre B.
Journal of the American Chemical Society, 2010 , vol. 132, # 37 p. 12817 - 12819
反应条件
palladium dichloride
0.0833333 h; microwave irradiation;
参考文献
Villemin, Didier; Elbilali, Abdelghani; Simeon, Fabrice; Jaffres, Paul-Alain; Maheut, Geraldine; Mosaddak, Mahjouba; Hakiki, Abdelhack
Journal of Chemical Research - Part S, 2003 , # 7 p. 436 - 437
反应条件
water; hydrogen cation
参考文献
Creary, Xavier; Benage, Brigitte; Mehrsheikh-Mohammadi, M. E.; Bays, J. Philip
Tetrahedron Letters, 1985 , vol. 26, # 20 p. 2383 - 2386
反应条件
1: NH3 / Irradiation
2: H(1+)/H2O
View Scheme
参考文献
Creary, Xavier; Benage, Brigitte; Mehrsheikh-Mohammadi, M. E.; Bays, J. Philip
Tetrahedron Letters, 1985 , vol. 26, # 20 p. 2383 - 2386
反应条件
water; hydrogen cation
参考文献
Issleib, K.; Doepfer, K.-P.; Balszuweit, A.
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 14, p. 171 - 178
反应条件
1: Pd(PPh3)4, triethylamine
2: H(+), water
View Scheme
参考文献
Issleib, K.; Doepfer, K.-P.; Balszuweit, A.
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 14, p. 171 - 178
