4,4-二甲氧基二苯基甲烷合成路线 (共 148 条)
反应条件
benzoyl chloride; pentacarbonyliron(0) in 1,3,5-trimethyl-benzene
Heating;
参考文献
Luh, Tien-Yau
Synthetic Communications, 1981 , vol. 11, # 10 p. 829 - 834
反应条件
1,3,2-benzodithiazole 1,1,3,3-tetraoxide; acetonitrile
2 h; Reflux;
参考文献
Barbero, Margherita; Bazzi, Stefano; Cadamuro, Silvano; Dughera, Stefano
European Journal of Organic Chemistry, 2009 , # 3 p. 430 - 436
反应条件
potassium hydroxide
Reduction; Wolff-Kishner reduction; 0.5 h; microwave irradiation;
参考文献
Gadhwal, Sunil; Baruah, Mukulesh; Sandhu, Jagir S.
Synlett, 1999 , # 10 p. 1573 - 1574
反应条件
silver tetrafluoroborate; di-n-propylmercury in dichloromethane
24 h; other reagent tetraethyltin;
参考文献
Reutov, O. A.; Uglova, E. V.; Mikhura, I. V.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1985 , vol. 34, # 4 p. 825 - 828
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1985 , # 4 p. 905 - 908
反应条件
zeolite in hexane
1 h; UV-irradiation;
参考文献
Clennan, Edward L.; Pan, Gui-Ian
Organic Letters, 2003 , vol. 5, # 26 p. 4979 - 4982
反应条件
1.1: 12 percent / pyridinium chlorochromate; celite / CH2Cl2 / 6 h
2.1: zeolite / hexane / 4 h / UV-irradiation
3.1: diethyl ether / 2 h / 20 °C
3.2: 66 percent / p-toluenesulfonic acid / benzene / 12 h / Heating
4.1: 38 percent / Zn(Hg); HCl / ethanol / 0.5 h / Heating
View Scheme
参考文献
Clennan, Edward L.; Pan, Gui-Ian
Organic Letters, 2003 , vol. 5, # 26 p. 4979 - 4982
反应条件
N,N-dimethyl acetamide
T=25°C;
参考文献
Streidl, Nicolas; Mayr, Herbert
European Journal of Organic Chemistry, 2011 , # 13 p. 2498 - 2506
反应条件
sulfuric acid; acetic acid
参考文献
Matsumura
Journal of the American Chemical Society, 1935 , vol. 57, p. 128
反应条件
in dichloromethane; water
T=60°C; 0.25 h;
参考文献
Gautret, Philippe; El-Ghammarti, Samira; Legrand, Anne; Couturier, Daniel; Rigo, Benoit
Synthetic Communications, 1996 , vol. 26, # 4 p. 707 - 713
反应条件
bromine in tetrachloromethane
Irradiationheating;
参考文献
Wei, Qiyan; Luo, Yinggang; Zhou, Min; Tao, Feiyan; Zhang, Guoling
Synthetic Communications, 2005 , vol. 35, # 6 p. 835 - 843