2-呋喃基(3-吡啶基)甲酮合成路线 （共 6 条）
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate in methoxybenzene
T=100°C; Suzuki carbonylative coupling; P=760.051 Torr; 20 h; chemoselective reaction;
参考文献
Li, Hongling; Yang, Min; Qi, Yanxing; Xue, Jijun
European Journal of Organic Chemistry, 2011 , # 14 p. 2662 - 2667
反应条件
chromium(VI) oxide in pyridine; water
100 h; Ambient temperature;
参考文献
Sauter, Fritz; Stanetty, Peter; Sittenthaler, Wilhelm; Waditschatka, Rudolf
Monatshefte fuer Chemie, 1988 , vol. 119, p. 1427 - 1438
反应条件
1: furan With n-butyllithium in diethyl ether
2 h; Heating;
2: pyridine-3-carbonitrile in diethyl ether
T=-78 - 20°C;
3: With hydrogenchloride in diethyl ether
参考文献
Chubb; Bryce; Tarbit
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 16 p. 1853 - 1854
反应条件
1: 1) 1.6M n-BuLi / 1) ether, n-hexane, 0 deg C, 2) ether, 1 h, -20 deg C; 1 h, 0 deg C
2: 19.3 percent / CrO3 / pyridine; H2O / 100 h / Ambient temperature
View Scheme
参考文献
Sauter, Fritz; Stanetty, Peter; Sittenthaler, Wilhelm; Waditschatka, Rudolf
Monatshefte fuer Chemie, 1988 , vol. 119, p. 1427 - 1438
反应条件
1: 1) 1.6M n-BuLi / 1) ether, n-hexane, 1 h, -60 deg C, 2) ether, 1 h, -25 deg C
2: 19.3 percent / CrO3 / pyridine; H2O / 100 h / Ambient temperature
View Scheme
参考文献
Sauter, Fritz; Stanetty, Peter; Sittenthaler, Wilhelm; Waditschatka, Rudolf
Monatshefte fuer Chemie, 1988 , vol. 119, p. 1427 - 1438
反应条件
1: 1) 1.6M n-BuLi / 1) ether, n-hexane, 1 h, -60 deg C, 2) ether, 1 h, -25 deg C
2: 19.3 percent / CrO3 / pyridine; H2O / 100 h / Ambient temperature
View Scheme
参考文献
Sauter, Fritz; Stanetty, Peter; Sittenthaler, Wilhelm; Waditschatka, Rudolf
Monatshefte fuer Chemie, 1988 , vol. 119, p. 1427 - 1438
