3-(1-磺酰基哌啶)-苯甲酸合成路线 （共 5 条）
反应条件
in dichloromethane T=0°C; 0.5 h;
参考文献
OXAGEN LIMITED
Patent: WO2009/93029 A1, 2009 ;
Location in patent: Page/Page column 39 ;
反应条件
water; sodium hydroxide in methanol T=20°C;
参考文献
WO2013/96744 A1, ;
Page/Page column 235 ;
反应条件
1: triethylamine / dichloromethane / 20 °C 2: sodium hydroxide; water / methanol / 20 °C View Scheme
反应条件
1: triethylamine / dichloromethane / 20 °C 2: sodium hydroxide; water / methanol / 20 °C View Scheme
反应条件
1.1: 1,1'-carbonyldiimidazole / tetrahydrofuran / 4 h / 0 °C
1.2: 1 h / 0 °C
2.1: trichlorophosphate / N,N-dimethyl-formamide / 1 h / 80 °C
3.1: sodium azide / N,N-dimethyl-formamide / 22 h / 20 °C
4.1: hydrogen / palladium 10 on activated carbon / methanol / 23 h / 20 °C
View Scheme
参考文献
Jitsuoka, Makoto; Nagase, Tsuyoshi; Sato, Nagaaki; Tsukahara, Daisuke
Patent: US2011/9622 A1, 2011 ;
