1-甲氧基-2-(甲氧基甲氧基)苯合成路线 （共 14 条）
反应条件
n-butyllithium; iodine in tetrahydrofuran T=-40°C;
参考文献
Cheng, Chen-Yu; Liou, Jing-Ping; Lee, Mei-Jing
Tetrahedron Letters, 1997 , vol. 38, # 26 p. 4571 - 4574
反应条件
Montmorillonite K 10 in benzene T=50°C; 1 h;
参考文献
Journal of Organic Chemistry, , vol. 66, # 11 p. 4097 - 4098
参考文献
Journal of the Chemical Society, , p. 102,104
反应条件
1: With n-butyllithium in tetrahydrofuran T=-78°C; 2 h; 2: With iodine in tetrahydrofuran T=-50 - 20°C;
参考文献
MERCK SHARP and; DOHME CORP.; LIU, Kun; STACHEL, Shawn J.; COBURN, Craig A.; STEELE, Thomas G.; SOLL, Richard; WU, Hao; PENG, Xuanjin; CAI, Yaxian; DU, Xiaoxing; LI, Jian
Patent: WO2010/94242 A1, 2010 ;
Location in patent: Example 3.2 ;
WO 2010/094242 A1
反应条件
1: 2-methoxy-phenol With potassium tert-butylate in tetrahydrofuran; N,N-dimethyl-formamide
T=20°C; 2 h;
2: chloromethyl methyl ether in tetrahydrofuran; N,N-dimethyl-formamide
T=20°C; 5 h;
参考文献
BANYU PHARMACEUTICAL CO., LTD.
Patent: EP1944301 A1, 2008 ;
Location in patent: Page/Page column 75-76 ;
EP 1944301 A1
反应条件
tin(IV)octabromotetraphenylporphyrinato trifluoromethanesulfonate
T=20°C; 0.166667 h;
参考文献
Moghadam, Majid; Tangestaninejad, Shahram; Mirkhani, Valiollah; Mohammadpoor-Baltork, Iraj; Khajehzadeh, Mostafa; Kosari, Farshid; Araghi, Mehdi
Polyhedron, 2010 , vol. 29, # 1 p. 238 - 243
反应条件
sodium acetate; silver trifluoromethanesulfonate in tetrahydrofuran
0.0833333 h; Ambient temperature;
参考文献
Marcune; Karady; Dolling; Novak
Journal of Organic Chemistry, 1999 , vol. 64, # 7 p. 2446 - 2449
反应条件
sodium hydride in diethyl ether
参考文献
Mabic; Vaysse; Benezra; Lepoittevin
Synthesis, 1999 , # 7 p. 1127 - 1134
参考文献
Birch
Journal of the Chemical Society, 1947 , p. 102,104
参考文献
Hoering; Baum
Patent: DE209608 ;
