in ethanol Irradiationdirect irradiation using 300-W Hg-lamp filtered by Corning CS-052 (>350 nm), with about 10-fold excess of dabco; Further byproducts given. Title compound not separated from byproducts;
sodium ethanolate in tetrahydrofuran; ethanol T=45°C; 5.5 h; similar further reactions of other related amidines (various reaction-times); Product distribution;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 38, # 3 p. 590 - 596
in ethanol IrradiationDirect irradiation using 300-W Hg-lamp filtered by Corning CS-052 (>350 nm).; Further byproducts given. Title compound not separated from byproducts;
in ethanol Irradiationdirect irradiation using 300-W Hg-lamp filtered by Corning CS-052 (>350 nm), with about 10-fold excess of dabco; Further byproducts given. Title compound not separated from byproducts;
Wai, Kwok-Fai; Sammes, Michael P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 1 p. 183 - 187