1-甲氧基-4-苯基乙炔苯合成路线 (共 169 条)
反应条件
(i), (ii) aq. HCl; Multistep reaction;
参考文献
Eisch,J.J.; Hordis,C.K.
Journal of the American Chemical Society, 1971 , vol. 93, # 12 p. 2974 - 2981
反应条件
sodium methylate; triphenylphosphine; palladium diacetate in methanol
T=25°C; 48 h;
参考文献
Wei, Li-Lan; Wei, Li-Mei; Pan, Wen-Bin; Leou, Shiow-Piaw; Wu, Ming-Jung
Tetrahedron Letters, 2003 , vol. 44, # 9 p. 1979 - 1981
反应条件
palladium diacetate; triphenyl silane in tetrahydrofuran
T=20°C; 7 h;
参考文献
Cacchi, Sandro; Fabrizi, Giancarlo; Goggiamani, Antonella; Persiani, Daniela
Organic Letters, 2008 , vol. 10, # 8 p. 1597 - 1600
反应条件
oxygen; potassium acetate; palladium diacetate in dimethyl sulfoxide
T=80°C; P=760.051 Torr; 24 h; Overall yield = 60 percent;
参考文献
Xu, Yun-He; He, Tao; Zhang, Qiu-Chi; Loh, Teck-Peng
Chemical Communications, 2014 , vol. 50, # 21 p. 2784 - 2786
反应条件
palladium dichloride in chlorobenzene
12 h; Reflux; Overall yield = 76 percent;
参考文献
Xie, Hou-Zhi; Gao, Qi; Liang, Ying; Wang, Heng-Shan; Pan, Ying-Ming
Green Chemistry, 2014 , vol. 16, # 4 p. 2132 - 2135
反应条件
dimethyl sulfoxide; PdI2
T=140°C; 2 h;
参考文献
Mousset, Celine; Provot, Olivier; Hamze, Abdallah; Bignon, Jerome; Brion, Jean-Daniel; Alami, Mouad
Tetrahedron, 2008 , vol. 64, # 19 p. 4287 - 4294
反应条件
lithium perchlorate in acetonitrile
9 h; anodic oxidation;
参考文献
Cariou, Michel
Tetrahedron, 1991 , vol. 47, # 4/5 p. 799 - 808
反应条件
anhydrous lithium nitrate in water; acetonitrile
Electrochemical reaction;
参考文献
Wille, Uta; Andropof, Jilliarne
Australian Journal of Chemistry, 2007 , vol. 60, # 6 p. 420 - 428
反应条件
hydroxytriphenylsilane; hexacarbonyl molybdenum in octane
0.166667 h; Irradiation;
参考文献
Villemin, Didier; Heroux, Michael; Blot, Virginie
Tetrahedron Letters, 2001 , vol. 42, # 22 p. 3701 - 3703