Co(2-ethylhexanoate)2-Al(C2H5)2; cobalt(II) 2-ethylhexanoate in toluene T=150°C; P=9880 Torr; 10 h; Yield given. Yields of byproduct given;
参考文献
Selimov, F. A.; Khafizov, V. R.; Dzhemilev, U. M.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1984 , vol. 20, # 3 p. 290 - 295
Khimiya Geterotsiklicheskikh Soedinenii, 1984 , vol. 20, # 3 p. 360 - 365
Fleming, Ian; Newton, Trevor W.; Roessler, Felix
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2527 - 2532
Et2NH; copper(l) iodide in tetrahydrofuran (Ar); CuI was added to suspn. of Pt complex in THF/Et2NH at 0°C; ethyne was bubbled through mixt. for 2 h; solvent removed (vac.); residue dissolved in CH2Cl2; washed (H2O); org. phase dried (MgSO4); filtered; filtrate passed through alumina; solvent removed; recrystd. (CH2Cl2/ether); dried (vac.);
参考文献
Janka, Mesfin; Anderson, Gordon K.; Rath, Nigam P.
Organometallics, 2004 , vol. 23, # 19 p. 4382 - 4390
