反应条件
1: 6,7-dihydroxy-3,4-dihydro-1(2H)-naphthalenone With cesium fluoride in N,N-dimethyl-formamide
T=20°C; deprotonation; 3 h;
2: 1,1-dibromomethane in N,N-dimethyl-formamide
T=100°C; Etherification; 2 h;
参考文献
Harayama, Takashi; Yasuda, Hirotake; Akiyama, Toshihiko; Takeuchi, Yasuo; Abe, Hitoshi
Chemical and Pharmaceutical Bulletin, 2000 , vol. 48, # 6 p. 861 - 864