sodium hydroxide; Aliquatreg; 336 in water T=10°C; 3 h;
参考文献
Sugawara, Akira; Hasegawa, Ken; Suzuki, Ken-ichi; Takahashi, Yukio; Sato, Ryu
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 435 - 437
n-butyllithium 1.) THF, -5-(-10) grad C, 30 min, nitrogen, 2.) THF, 1 h at -5-(-10) grad C then 24 h at room temp.; Yield given. Multistep reaction. Yields of byproduct given;
Bowen, D. Richard; Maccoll, Allan
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1985 , p. 1101 - 1104
iodine 1.) THF, RT, 2.) a) -78 deg C, 3 h, b) RT, 3 h; Yield given. Multistep reaction;
参考文献
Rieke, Reuben D.; Schulte, Louis D.; Dawson, Bryan T.; Yang, Sheng Sbeng
Journal of the American Chemical Society, 1990 , vol. 112, # 23 p. 8388 - 8398
