1-二乙氧基磷酰-2-甲基丙烷-1-醇合成路线 （共 5 条）
反应条件
DBN
T=180°C; Abramov reaction; 0.025 h; Microwave irradiationneat (no solvent);
参考文献
Kabachnik; Minaeva; Beletskaya
Russian Journal of Organic Chemistry, 2009 , vol. 45, # 8 p. 1119 - 1122
反应条件
chloro-trimethyl-silane; lithium perchlorate in diethyl ether
T=20°C; 0.0833333 h;
参考文献
Azizi, Najmedin; Saidi, Mohammad R.
Phosphorus, Sulfur and Silicon and the Related Elements, 2003 , vol. 178, # 6 p. 1255 - 1259
反应条件
hydrogenchloride in diethyl ether; dichloromethane
T=-10°C; 1 h;
参考文献
Goldeman, Waldemar; Soroka, Miroslaw
Synthesis, 2006 , # 18 p. 3019 - 3024
反应条件
N'''-tert-butyl-N,N,N',N',N'',N''-hexamethylphosphorimidic triamide in diethyl ether
20 h; Ambient temperature;
参考文献
Drescher; Hammerschmidt; Kahlig
Synthesis, 1995 , # 10 p. 1267 - 1272
反应条件
tris-(2-chloro-ethyl)-amine; triphenylphosphine; diethylazodicarboxylate in benzene
5 deg C, 30 min to r.t., 20 h;
参考文献
Gajda; Matusiak
Synthesis, 1992 , # 4 p. 367 - 368
