5-甲基-2-苯基苯并恶唑合成路线 （共 48 条）
反应条件
1: K2CO3; [PdCl2(PPh3)2]; CuI / dimethylformamide / 90 °C / 760 Torr
2: P2O5; TsOH*H2O / dimethylformamide / 3 h / 120 °C
View Scheme
参考文献
Zhou; Chen
Journal of Chemical Research - Part S, 2001 , # 6 p. 235 - 237
反应条件
diethyl-1,4-dihydro-2,6-dimethyl-3,5-pyridine dicarboxylate; 10 palladium on activated carbon in acetic acid
T=120°C; 15 h; Inert atmosphere;
参考文献
Xing, Rui-Guang; Li, Ya-Nan; Liu, Qiang; Meng, Qing-Yuan; Li, Jing; Shen, Xiao-Xia; Liu, Zhengang; Zhou, Bo; Yao, Xiaojun; Liu, Zhong-Li
European Journal of Organic Chemistry, 2010 , # 34 p. 6627 - 6632
反应条件
H14[NaP5W30O110]
T=90°C; 0.25 h; Neat (no solvent);
参考文献
Heravi, Majid M.; Javanmardi, Najme; Oskooie, Hossein A.; Baghernejad, Bita; Heidari, Maryam; Bamoharram, Fatemeh F.
Journal of the Chinese Chemical Society, 2009 , vol. 56, # 3 p. 589 - 593
反应条件
(Ru2(η5-C5Ph4O)2(H)2(CO)4); 2,6-dimethoxy-p-benzoquinone; bis(salicylideniminato-3-propyl)methylamino-cobalt(II) in chlorobenzene
T=120°C; 24 h;
参考文献
Endo, Yoshinori; Baeckvall, Jan-E.
Chemistry - A European Journal, 2012 , vol. 18, # 43 p. 13609 - 13613
反应条件
oxygen; caesium carbonate; silver carbonate; bis(dibenzylideneacetone)-palladium(0) in dimethyl sulfoxide; N,N-dimethyl-formamide
T=140°C; 11 h;
参考文献
Liu, Dongfang; Liu, Bin; Cheng, Jiang
RSC Advances, 2013 , vol. 3, # 24 p. 9193 - 9196
反应条件
oxygen; potassium carbonate in chloroform; water
T=30°C; P=760.051 Torr; 20 h;
参考文献
Yoo, Woo-Jin; Yuan, Hao; Miyamura, Hiroyuki; Kobayashi, Shu
Canadian Journal of Chemistry, 2012 , vol. 90, # 3 p. 306 - 313
反应条件
potassium carbonate in water; chlorobenzene
T=140°C; 12 h; Sealed tube;
参考文献
Wang, Lei; Ren, Xinyi; Yu, Jintao; Jiang, Yan; Cheng, Jiang
Journal of Organic Chemistry, 2013 , vol. 78, # 23 p. 12076 - 12081
反应条件
1: With CM-phos; palladium diacetate; potassium carbonate; triethylamine
Inert atmosphere;
2: in N,N-dimethyl-formamide; tert-butyl alcohol
T=110°C; 24 h; Inert atmosphere;
参考文献
So, Chau Ming; Lau, Chak Po; Kwong, Fuk Yee
Chemistry - A European Journal, 2011 , vol. 17, # 3 p. 761 - 765
反应条件
dipotassium peroxodisulfate; 1,10-phenanthroline; palladium diacetate in dimethyl sulfoxide; toluene
T=120°C; 24 h; air; chemoselective reaction;
参考文献
Li, Chengliang; Li, Pinhua; Yang, Jin; Wang, Lei
Chemical Communications, 2012 , vol. 48, # 35 p. 4214 - 4216
反应条件
iron(III) sulphate hydrate; oxygen; RF-PPh3 in diethylene glycol dimethyl ether; water
T=110°C; 36 h; Sealed tube;
参考文献
Liu, Saiwen; Chen, Ru; Guo, Xiangyu; Yang, Huiqiong; Deng, Guojun; Li, Chao-Jun
Green Chemistry, 2012 , vol. 14, # 6 p. 1577 - 1580
