(2,2-二溴乙烯基)苯合成路线 （共 99 条）
反应条件
1,4-diaza-bicyclo[2.2.2]octane in 1-methyl-2-pyrrolidinone T=100°C;
参考文献
Shen, Wang; Kohn, Todd; Fu, Zice; Jiao, XianYun; Lai, Sujen; Schmitt, Michael
Tetrahedron Letters, 2008 , vol. 49, # 51 p. 7284 - 7286
反应条件
copper(l) iodide; tetrabutyl ammonium fluoride; N-methyl-2-(methylamino)ethylamine in water; N,N-dimethyl-formamide T=65°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Xu, Hui; Zhang, Yin; Huang, Jianqiang; Chen, Wanzhi
Organic Letters, 2010 , vol. 12, # 16 p. 3704 - 3707
反应条件
1: 1,1-dibromostyrene With n-butyllithium T=-78°C; Corey-Fuchs reaction; 2: N,N-dimethyl-formamide Corey-Fuchs reaction; 3: With potassium dihydrogenphosphate; water Corey-Fuchs reaction;
参考文献
Zheng, Weihong; Degterev, Alexei; Hsu, Emily; Yuan, Junying; Yuan, Chengye
Bioorganic and Medicinal Chemistry Letters, 2008 , vol. 18, # 18 p. 4932 - 4935
反应条件
Pd0(tris(tert-butyl)phosphine)2; cesium fluoride in 1,4-dioxane T=60°C; 24 h; Schlenk techniqueInert atmosphere; Temperature;
参考文献
Shimizu, Masaki; Nagao, Ikuhiro; Kiyomoto, Shin-Ichi; Hiyama, Tamejiro
Australian Journal of Chemistry, 2012 , vol. 65, # 9 p. 1277 - 1284,8
Title/Abstract Full Text Show Details
Shimizu, Masaki; Nagao, Ikuhiro; Kiyomoto, Shin-Ichi; Hiyama, Tamejiro
Australian Journal of Chemistry, 2012 , vol. 65, # 9 p. 1277 - 1284
反应条件
aluminum oxide; potassium fluoride; copper(l) iodide; triphenylphosphine; nickel 0.05 h; microwave irradiation;
参考文献
Journal of Chemical Research, , # 1 p. 71 - 73
反应条件
potassium phosphate; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide T=90°C; 2 h; Inert atmosphere;
参考文献
Rao, Maddali L. N.; Jadhav, Deepak N.; Dasgupta, Priyabrata
Organic Letters, 2010 , vol. 12, # 9 p. 2048 - 2051
反应条件
copper(l) iodide; potassium iodide in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=120°C; 12 h;
参考文献
Suzuki, Hitomi; Aihara, Mie; Yamamoto, Hidetoshi; Takamato, Yuuko; Ogawa, Takuji
Synthesis, 1988 , # 3 p. 236 - 238
反应条件
potassium phosphate; copper(l) iodide; 8-hydroxy-quinoline in ethanol T=100°C; Suzuki Coupling; 12 h; Schlenk techniqueInert atmosphere;
参考文献
Liu, Jidan; Dai, Fenglin; Yang, Zhiyong; Wang, Sizhuo; Xie, Kai; Wang, Anwei; Chen, Xiang; Tan, Ze
Tetrahedron Letters, 2012 , vol. 53, # 42 p. 5678 - 5683
反应条件
copper(l) iodide; N,N,N',N,-tetramethylethylenediamine; caesium carbonate in 1,4-dioxane T=102°C; 24 h; Inert atmosphere;
参考文献
Synlett, , # 4 p. 589 - 594
反应条件
N,N,N',N,-tetramethylethylenediamine; caesium carbonate; copper(II) oxide in 1,4-dioxane T=80°C; 24 h; Inert atmosphere;
参考文献
Wang, Man-Gang; Wu, Jun; Shang, Zhi-Cai
Synlett, 2012 , # 4 p. 589 - 594
