in tetrahydrofuran; THF-d8 (tetrahydrofuran-d8) absence of air and moisture; slow addn. of Ga-compd. (in THF-d8) to naphthalenide soln. (prepd. by stirring Li and naphthalene in THF), stirring (-78°C, 30 min), then standing for 25 d at room temp.; not isolated, reaction followed by (1)H-NMR spectroscopy;
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Gmelin Handbook: B: B-Verb.8, 11.2.3, page 167 - 173
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Moore, C. E.; Cassaretto, F. P.; McLafferty, J. J.; Posvic, H. W.
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