反应条件
in diethyl ether byproducts: H2; High Pressure; Mg powder and Et2O put into stainless steel autoclave; sealed and maintained at 600°C for 12 h; cooled to room temp. naturally; collected; washed with pure ethanol, dilute HCl and distilled water several times; dried in vacuum at 60°C for 6 h;
参考文献
Chemistry Letters, , vol. 34, # 2 p. 168 - 169
