potassium chloride in melt
at 800-1000°C 60 min, form of product is powder; chlorids dissolve water after cooling;
参考文献
Lefever, R. A.
Journal of the Electrochemical Society, 1961 , vol. 108, p. 107 - 108
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Gmelin Handbook: Ni: MVol.AI, 10.2, page 609 - 616
Boullee, A.; David, R.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1956 , vol. 243, p. 495 - 498
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Gmelin Handbook: Ni: MVol.AI, 10.1, page 603 - 609
hydrogen in water
at 300°C and 180 atm for about 17.5 h;; final product: 77percent NiO and 23percent Ni (approx.);;
参考文献
Ipat'ev, V. N.; Kondyrev, I. N.
Ber. Dtsch. Chem. Ges., 1926 , vol. 59, p. 1421 - 1422
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Ipat'ev, V. N.; Kondyrev, I. N.
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, 1926 , vol. 58, p. 692 - 698
in diethyl ether
byproducts: Mg(acac)(PhC(NTMS)2), C2H6; (exclusion of oxygen and moisture); Mg complex added to a soln. of Ni complex at -30°C, warmed to -10°C, stirred at this temp. for4 h; evapd., toluene added, filtered, crystd. for 1 wk at -40°C;
参考文献
Nelkenbaum, Elza; Kapon, Moshe; Eisen, Moris S.
Organometallics, 2005 , vol. 24, # 11 p. 2645 - 2659
