in further solvent(s)
Ni complex (0.5 g) and oleylamine (5 ml) heated (150°C, 60 min) under Ar; injected into PPh3 (5 g) (245°C); aged (235°C, 40min); cooled to room temp.; pptd. with EtOH; washed with EtOH; dried (100°C); TEM;
参考文献
Davar, Fatemeh; Fereshteh, Zeinab; Salavati-Niasari, Masoud
Journal of Alloys and Compounds, 2009 , vol. 476, # 1-2 p. 797 - 801
in neat (no solvent)
byproducts: H2O, CO2, CO; heated at heating rate of 10°C/min under He gas flow to 600°C; monitored by X-ray diffraction;
参考文献
Rejitha; Mathew, Suresh
Journal of Thermal Analysis and Calorimetry, 2010 , vol. 102, # 3 p. 931 - 939
→
反应条件
in melt
byproducts: H2;
参考文献
Kirsebom, G. N.
Tidsskr. Kjemi Bergves., 1940 , vol. 20, p. 1 - 7
C., 1940 , vol. II, p. 813
Full Text Show Details
Kirsebom, G. N.
Tidsskr. Kjemi Bergves., 1940 , vol. 20, p. 1 - 7
C. A., 1941 , p. 7331
in neat (no solvent)
equilibrium at 1100 - 1300°C;;
参考文献
Hahn, W. C.; Muan, A.
Physics and Chemistry of Solids, 1961 , vol. 19, p. 338 - 348
Full Text View citing articles Show Details
Gmelin Handbook: Ni: MVol.B3, 153, page 1110 - 1112
Kirsebom, G. N.
Patent: GB351653 , 1931 ;
C., 1931 , vol. II, p. 2210
Full Text Show Details
Kirsebom, G. N.
Tidsskr. Kjemi Bergves., 1940 , vol. 20, p. 1 - 7
C. A., 1941 , p. 7331
