反应条件
in methanol; pentane byproducts: C5(CH3)4(H)CH2OCH3, (C10(CH3)8(CH2OCH3)2)Fe; Ar atmosphere, dry solvents; Na-methoxide (from Na) in MeOH, pentane andMeOH soln. of Fe-compd. addn., shaking (5-7 min), lower (MeOH) layer re peatedly extracting with pentane; pentane extracts combining, residue drying (5 torr), residue extracting (pentane), chromy. (Al2O3, pentane); elem. anal.;
参考文献
Russian Chemical Bulletin, , vol. 47, # 12 p. 2451 - 2454
