反应条件
butyl bromide in neat (no solvent, gas phase) cocondn. on surface cooled with liq. nitrogen (reaction vessel (vac. ca. 1E-5 mm) in Dewar vessel, tin atomization with STP-30 stabilized powersupply, proportion of Sn:alkyl halide vapor 1:10 to 1:1000),reaction vessel removal from Dewar vessel; reaction mixt. dissoln. (ethanol), soln. filtration, alcohol transcondn. (vac.), powder exposing to vac. for several d; elem. anal.;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 52, p. 2283 - 2287
Zhurnal Obshchei Khimii, , vol. 52, p. 2583 - 2588