in melt Kinetics; placing of mixt. of Ti with SnF2 (molar ratio SnF2:Ti=4.04) in Fluoroplast-4 ampule, closing by screwed stopper, exposition for 1.00 h at 230°C; various product ratio yields for various conditions; cooling, stirring up in water, collection, drying;
参考文献
Goryacheva; Rakov; Solov'ev
Russian Journal of Inorganic Chemistry, 2001 , vol. 46, # 7 p. 949 - 952
Botts, E. D.; Krauskopf, F. C.
Journal of Physical Chemistry, 1927 , vol. 31, p. 1404 - 1409
Full Text Show Details
Gmelin Handbook: Ti: MVol., 3.5, page 189 - 199
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反应条件
in neat (no solvent) equimolar mixt. fusing (vac. arc furnace, tungsten electrode); optical microscopy;
参考文献
Vasyutinskii, N. V.; Rys'eva, Yu. I.
Russian Journal of Inorganic Chemistry (Translation of Zhurnal Neorganicheskoi Khimii), 1978 , vol. 23, p. 621 - 623
Zhurnal Neorganicheskoi Khimii, 1978 , vol. 23, p. 1122 - 1126
