Fisher
Annalen der Physik (Weinheim, Germany), 1826 , vol. 8, p. 499
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Fisher
Annalen der Physik (Weinheim, Germany), 1827 , vol. 9, p. 264
NaBH4 in tetrahydrofuran; dimethyl sulfoxide byproducts: NaCl, BH3, hydrogen; (Ar); reflux of Zn and NaBH4 in THF under stirring for 0.5 h, quick injecting of soln. of SbCl3 in THF, reflux at 75°C for 24 h, addn. ofDMSO; heating at 190°C;
参考文献
Journal of Solid State Chemistry, , vol. 183, # 5 p. 1090 - 1094
