Gromov, S. I.; Kataev, G. A.
Trudy Tomskogo Gosudarstvennogo Universiteta, 1962 , vol. 154, p. 128 - 131
C. A., 1964 , vol. 60, p. 5324
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Gmelin Handbook: C: MVol.D2, 4.1.2.7.7.12, page 241 - 241
in acetonitrile Electrolysis; 4 h, initial voltage 10 V, Zn anode; product was collected, washed with acetonitrile and then petroleum ether and dried in vacuo; elem. anal.;
参考文献
Geloso, Corrado; Kumar, Rajesh; Lopez-Grado, Jaime Romero; Tuck, Dennis G.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 928 - 932
water in further solvent(s) byproducts: C6H5Cl; Sonication; (N2); solvent = 1,1,3,3-tetramethylurea contg. water; 2 equivs. of Zn powder used; 30 °C, ultrasound applied for 8 h; 100percent conversion; not isolated; conversion and yield detd. by quenching with I2;
nBu4NPF6 in acetylacetone Electrochem. Process; tetra-n-butylammonium hexafluorophosphate added to dry acetylacetone, Cuelectrode, 300 V, 10-50 mA, ca. 10 h; solid filtered off, washed twice with hexane and with petroleum ether;
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Synthesis and Reactivity in Inorganic, Metal-Organic and Nano-Metal Chemistry, , vol. 37, # 10 p. 813 - 815
tetraethylammonium chloride in acetonitrile byproducts: hydrogen; Electrolysis; electrolyis of Hacac and ZnCO3 in temp.-controlled electrochem. cell equipped with Zn anode and cathode for 193 min; using 0.1 M soln. of Et4NClin MeCN as electrolyte; concn. to pasty state under heating on magnetic stirrer and cooling to room temp.; extn. with ether; filtration, concn. of filtrate; elem. anal.;
参考文献
Russian Journal of Inorganic Chemistry, , vol. 52, # 4 p. 577 - 580
