triphenylphosphine in tetrahydrofuran; acetonitrile
byproducts: ZnCl2; N2-atmosphere; refluxing 3 equiv. of PPh3 with PdCl2 (1 h), addn. of Zn-dust, refluxing for 5 h; hot filtration, crystn. on cooling to room temp., washing (EtOH), drying(vac.); elem. anal.;
参考文献
Giannoccaro, P.; Sacco, A.; Vasapollo, G.
Inorganica Chimica Acta, 1979 , vol. 37, p. L455 - L456
in xylene
on react. of diaryl mercury compd. with Zn wool in anhyd. xylene;;
参考文献
Kozeschkow, K. A.; Nesmeyanow, A. N.; Potrosov, W. I.
Ber., 1934 , vol. 67, p. 1138 - 1142
Show Details
Gmelin Handbook: Zn: SVol., 177, page 555 - 558
