in tetrahydrofuran
(CH3C5H4)TiCl2(THF) prepd. in THF by the method of Lucas,C.R. and Green,M.L.H, Inorg. Synth. 16(1976)237; ((CH3)3Si)2S added to the soln.; stirring for 18 h under nitrogen; solvent removed in vac., residue extd. with hot hexane; filtrate concd. to a small volume and cooled to -25° overnight; elem. anal.;
参考文献
Darkwa, James; Lockemeyer, John R.; Boyd, Peter D. W.; Rauchfuss, Thomas B.; Rheingold, Arnold L.
Journal of the American Chemical Society, 1988 , vol. 110, # 1 p. 141 - 149
