反应条件
in dichloromethane under N2, 3 equiv. of Li-compd., 1 equiv. of Bi-compd. and 5 equiv. of C6Me6 were stirred in CH2Cl2 for 4 h; soln. was concd., held at -24 °C for 2 weeks. soln. was filtered,concd., held at -24 °C for 3 weeks, crystals were sepd. by manua lly, Bi-contg. and not-Bi-contg. products ratio was. 3:1, elem. anal.;
参考文献
Polyhedron, , vol. 24, # 18 p. 2994 - 3003
