in neat (no solvent) byproducts: Al2O3; AlI3 was heated with TeO2 at 230°C for 24 h under reduced pressure;; isolation of TeI4: sublimation at 235°C;;
参考文献
Chaigneau, M.
Bulletin de la Societe Chimique de France, 1957 , p. 886 - 888
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Gmelin Handbook: Te: SVol.B1, 2.2.8.4, page 58 - 72
Oppermann, H.; Kunze, G.; Wolf, E.; Kokovin, G. A.; Sitschova, I. M.; Osipova, G. E.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1980 , vol. 461, p. 165 - 172
in methanol byproducts: H2O; addn. of dithiocarbamic acid (prepd. in situ) to suspn. of TeO2 (0°C)(molar ratio 4:1), stirring (5 h, room temp.); filtration, evapn. in vac.;
